poormanschemist

In this video I discuss the organic chemistry of amphetamines from a purely theoretical perspective. This is not a how-to video. There are no instructions on how to build meth labs or anything like that. This is just a discussion of the chemistry of these compounds. That's it.

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Reference 1: Reduction of Benzylic Alcohols and α-Hydroxycarbonyl Compounds by Hydriodic Acid in a Biphasic Reaction Medium by Michael Dobmeier, Josef M. Herrmann, Dieter Lenoir and Burkhard König. Bielstein Journal of Organic Chemistry.
https://www.beilstein-journals.org/bjoc/content/pdf/1860-5397-8-36.pdf
Reference 2: Video Essay on the Chemistry of Tryptamines:
https://www.bitchute.com/video/1YROZVK3PqCB/

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IT WORKED!!! In this video I carry out a reduction of BaSO4 to BaS using nothing more than sugar carbon, a tiny bit of water, and a couple hours of heating. To prove the reaction worked I used the BaS solution I obtained to precipitate out barium carbonate on addition to aqueous Na2CO3 and barium sulfate plus hydrogen sulfide gas on addition of aqueous sulfuric acid. Now we have a way to turn ALL alkaline earth metal sulfates into something useful!!!

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In this video I prepare selenium tetrachloride from selenium metal and chlorine gas in concentrated HCl, I then use the stock solution of selenium tetrachloride to produce cesium hexachloroselenate and ammonium hexachloroselenate. Both products are very reactive with water and moisture so I stored them under the solutions they were precipitated from.

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In this video I finally conquer potassium octacyanomolybdate using a prep from a paper from 1974. In this prep potassium molybdate dihydrate K2MoO4 (made from ammonium molybdate and KOH) is reduced with potassium borohydride and glacial acetic acid in the presence of sodium potassium cyanide (made in the usual way). It still threw me some pretty wicked curve balls like the final product being obtained as an oil that had to air dry; didn't see that one coming. But in the end I obtained a nice, bright yellow product exactly as described in the literature! See? Hard work and perseverance really does pay off!!!

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Stoichiometric Calculations:
http://www.poormanschemist.com/PMC_Notebook/JanJun2021/PMC_LabNotebook_JanJun2021.html

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In this video I prepare the acetylacetonato complex of thorium(IV) from thorium sulfate, 2,4-pentanedione (aka acetylacetone), and potassium hydroxide. The crude product is recrystallized from hot ethanol by the addition of a small amount of a very dilute solution of KOH. The process for this prep comes from the atomistry article for thorium acetylacetonate and can be found here:
http://thorium.atomistry.com/thorium_acetylacetone.html

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In this video I attempted a prep of telluric acid from tellurium and chloric acid as described in the Handbook of Preparative Inorganic Chemistry page 452. However, I ended up getting TeO2 instead. I'm still calling this a win because this turned out to be a VASTLY superior way of making TeO2 than anything else I have ever tried. And TeO2 is a common precursor for other Te compounds.

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In this first of its kind pre-experiment video I lay out the groundwork for how we will be doing the experiment as well as discussing astrology; a topic so intertwined with alchemy that we simply cannot neglect covering it if we wish to create an authentic alchemical product. It doesn't matter if we believe astrology has any bearing on reality. The ancients did. MUCH in alchemy will remain totally mysterious without a solid grounding in classical astrology. I barely even scratch the surface in this video but it is enough for you, dear viewer, to make sense of the experiment when we carry it out. :-)

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In this video I lay out the plan for my exodus from YouTube. I am not going to continue to generate traffic for a website that won't let me express a valid opinion. The YouTube channel will still exist but every video will just be a clip announcing when a video has been uploaded here. No more content for YouTube. I am working on expanding onto Odysee and reviving the Subscribe Star account (a lot of the stuff on there is posted publicly; you don't need to be a donor to see it). It's time to move on because I REFUSE to be cucked by the likes of Susan and her soy swilling minions!!!

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In this video I utterly destroy the "trust the science" mantra of the soy swilling retards that for some reason think that they have all the answers when in reality they are dumber than a box of fucking rocks! Although that's probably insulting to both the rocks and they box they're in.

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In this video I prepare barium sulfide from iron, sulfur, and barium hydroxide octahydrate. There were some hiccups along the way but in the end I was able to get a good product that seems to be largely free of barium carbonate.

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Download a Free Copy of Inorganic Laboratory Preparations:
https://1lib.us/book/666160/f02534

In this video I make some observations on being a chemistry content creator on the internet and I share some lessons I've learned along the way.

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In this video I carry out the synthesis portion of the prep of potassium octacyanomolybdate. Part 2 will be the purification of the crude product. However, I was able to confirm that the prep did work by obtaining a yellowish precipitate on reacting the crude solution with cadmium chloride solution.

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Free Download Inorganic Laboratory Preparations:
https://1lib.us/book/666160/f02534
Scaled Down Prep:
http://www.poormanschemist.com/PMC_Blog/PMC_Blog.html

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In this video the extremely problematic camera that I have been using up until recently that could never focus properly gets the fiery justice it so richly deserves.

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In this video I make the acetylacetonate of nickel(II) using nickel(II) nitrate hexahydrate, 2,4-pentanedione (acetylacetone), and sodium hydroxide. I had a few problems with this prep but in the end everything worked out fine. This prep is really easy to do and would be a good one for an amateur chemist who was just getting into tinkering with transition metal complexes.

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Download Inorganic Syntheses Volume 35:
https://1lib.us/book/2153269/de2b3a
See the prep in its entirety on my website:
http://www.poormanschemist.com/PMC_Blog/PMC_Blog.html

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In this short video I captured a timelapse of HgBr2 crystallizing from solution. I made the HgBr2 by reacting mercurous nitrate with elemental bromine and HBr. The video compresses a little over an hour into about 2 3/4 minutes.

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In this video I prepare beautiful crystals of pure mercuric chloride by bubbling chlorine gas through a suspension of 20.95 grams of mercurous chloride in water.

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In this video I make up a well known mercury compound that used to be called "fusible white mercuric precipitate" because this compound will melt unlike "infusible white mercuric precipitate" which was HgNH2Cl. This prep is fast, high yield, and very easy to carry out as it only takes HgCl2, dry ammonia gas, and anhydrous ethyl acetate.

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Download Inorganic Laboratory Preparations:
https://1lib.us/book/666160/f02534
Download Handbook of Preparative Inorganic Chemistry
https://1lib.us/book/557099/fc4586

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In this video I try to encourage a massive ant colony to vacate my yard by means of a popular pyrotechnic incendiary mix that is ignited by water.

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How to Make Workable Negative X:
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In this video I try out an experiment based on an atomistry article to try to produce barium ferrocyanide.

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This is a prep that is ideal for beginners. All that is needed is chromium(III) chloride hexahydrate, ammonium thiocyanate, and absolute ethanol. And it's reddish-purple. What more could you ask for? :-)

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Synthesis of Potassium Hexathiocyanatochromium(III):
https://www.bitchute.com/video/OHxfwg2KWL1F/
Download a free copy of Inorganic Laboratory Preparations:
https://1lib.us/book/666160/f02534

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In this video I prepare barium potassium osmocyanide from barium osmate that I made in a previous video. Addition of HCl followed by warming produces osmium(II) cyanide. This prep generated HCN gas and osmium readily forms a very dangerous tetroxide gas. This experiment is for experienced chemists only.

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Preparation of Barium Osmate:
https://www.youtube.com/watch?v=M5X_tLinRwo

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In this video I make ruthenium(II) cyanide from the barium potassium ruthenocyanide I made in the last video. This is a dangerous prep and should only be repeated by advanced chemists who are competent enough in their lab technique to deal with HCN gas.

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Atomistry Article on Potassium Ruthenocyanide:
http://ruthenium.atomistry.com/potassium_ruthenocyanide.html

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In this video I prepare ruthenocyanide and ruthenium purple from barium ruthenate and sodium potassium cyanide.

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Making Barium Ruthenate:
https://www.youtube.com/watch?v=gV2N2Jqpo6w
Ruthenocyanide Atomistry Article:
http://ruthenium.atomistry.com/potassium_ruthenocyanide.html

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The last few experiments that I've tried haven't worked out but this one did. So to hold you over until a real prep works here is the very weird compound cesium tetrachloronickelate(II).

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By popular demand in this video I repeat Chem Players experiment to prepare a mixed CN of sodium and potassium. This prep is fairly dangerous and should only be attempted by experienced chemists who are well grounded in practical lab work.

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Chem Player Original Video: https://www.bitchute.com/video/9rameiGenclD/

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Created 1 year, 8 months ago.

206 videos

Category Science & Technology

On this channel I focus on making rarely seen chemical compounds and demonstrating other laboratory procedures in my back yard chem lab. Unlike many home chemists I am not big on boom compounds. Instead I like to focus on those elements and compounds best described as "wildly poisonous" that other chemists hesitate to play with. I have a Bachelors degree in chem so yes I do know what I am doing. Although much of my stuff is not really meant for other amateur chemists to repeat (especially not a beginner!!!) I am very active in the amateur/hobby chemistry and I try to be as supportive of amateur chemists as I possibly can.
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