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Attempting Uncle Fester's HI Synthesis from I2 and Red Phosphorus in Water/Toluene Part 2

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First published at 05:30 UTC on January 13th, 2020.

poormanschemist

PoorMansChemist

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Distilling the product of the reaction done in the previous video after leaving it to sit overnight. Eventually I ended up with some azeotropic hydriodic acid. Not really sold on this as a great method for producing HI. Sure it works but honestly yo…

Uncle Fester's SoMM 7th Edition (free download from ZLibrary): https://b-ok.cc/book/830200/84d9b6
Preparation of Hydriodic Acid: https://www.prepchem.com/synthesis-of-hydroiodic-acid/
Iodine Solubility Data: https://onlinelibrary.wiley.com/doi/10.1002/047084289X.ri005

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