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Synthesis of Cobalt(II) Tetrathiocyanatomercurate(II) aka Mercury(II) Tetrathiocyanatocobaltate(II)

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First published at 00:23 UTC on March 9th, 2020.

#tetrathiocyanatocobaltate
#tetrathiocyanatomercurate
#mercury

poormanschemist

PoorMansChemist

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In this video I first synthesize a solution of mercuric nitrate from mercuric oxide and nitric acid. I then precipitate out mercuric thiocyanate. The potassium nitrate solution is decanted, the solid is washed, and then combined with another solution of potassium thiocyanate before being boiled. This produces a solution of potassium tetrathiocyanatomercurate(II). I then add a solution of cobalt chloride to precipitate out cobalt tetrathiocyanatomercurate(II). As I was making the video I found some online discussions that pointed to cobalt tetrathiocyanatomercurate and mercury tetrathiocyanatocobaltate being the same compound. I found an a prep video of mercury tetrathiocyanatocobaltate so I could compare that compound with the product of my synthesis. They were identical in appearance.

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Colorful Chemistry Cobalt Tetrathiocyanatomercurate Video:
https://www.youtube.com/watch?v=jUqjZziourY
Dr Krishna Swami G Mercury Tetrathiocyanatocobaltate Video:
https://www.youtube.com/watch?v=AgBttg89QOA
Handbook of Preparative Inorganic Chemistry Free Download:
https://b-ok.cc/book/436750/7efac2

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