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GRIGNARD REACTION propanoic acid synthesis PART 1

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First published at 14:09 UTC on February 1st, 2019.

#grignard
#propanoate
#propanoic

JBSC

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Ether is flammable so do not do this around any flames or pilot lights etc.........Basically i already got my grignard reagent i made in a previous video called "ethylmagnesium bromide (grignard reagent) synthesis. SO in this video (part 1) i am bubbling ANHYDROUS CO2 in to the grignard reagent to make my tetrahedral intermediate which is an alkoxide salt. Part 2 i will finish up and then quench the reaction to make the propanoic acid. And then i will extract it out with several washings with diethyl ether. Which will remove the POLAR impurities. Part 3 i will base the ether/propanoic acid mixture to make sodium propanoate and therefor remove the NON POLAR impuirities. Part 4 i will acidify again and make the proanoic acid and then use ether to extract it from the water. Dry with CaCl2. Then distill off the ether to have some what pure and anhydrous propanoic acid that i can distill out at 141 C.

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