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Synthesis of Cadmium(II) Iodide From Amorphous Cd and I2 in H2O

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First published at 22:38 UTC on February 18th, 2020.

poormanschemist

PoorMansChemist

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In this video I first carry out a preparation of amorphous cadmium metal from cadmium sulfate using a magnesium rod. The amorphous cadmium is taken and refluxed with iodine in water until all of the cadmium dissolves. The solution is then evaporated down over boiling water to both expel excess I2 and to crystallize the product. The cadmium(II) diiodide is then allowed to evaporate to dryness in a vacuum desiccator.

Inorganic Laboratory Preparations by Gert Schlessinger, PhD., Chemical Publishing Company, Inc., 1962. Pages 18-19. Free download at:
https://b-ok.cc/book/666160/f02534
Wikipedia Article for Cadmium(II) Iodide:
https://en.wikipedia.org/wiki/Cadmium_iodide

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Category	Science & Technology
Sensitivity	Normal - Content that is suitable for ages 16 and over

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