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In this video I make up pyridinium tribromide from pyridine, conc. HBr, Br2, in water. This compound is a useful reagent in organic chemistry and could prove to be a useful tool if one chose to research this compound and ones like it further.

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In this video I prepare the lead analog of ammonium hexachloroplatinate from lead(II) chloride, chlorine gas, and ammonium chloride. The prep turned out to be extremely easy to do and not nearly as difficult as the literature makes it seem like it would be. It would be a good prep for an intermediate level amateur chemist who is comfortable working with chlorine gas and soluble lead salts (both of which can be deadly). Ammonium hexachloroplumbate decomposes in water to PbCl2, Cl2, and NH4Cl but it is soluble without decomposition in 20% HCl,

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Download Handbook of Preparative Inorganic Chemistry:
https://b-ok.cc/book/436750/7efac2
Download Inorganic Laboratory Preparations:
https://b-ok.cc/book/666160/f02534

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In this video I prepare BPSP following a prep published by the Chem Department of Shiraz University, Iran (Tetrahedron Letters, Vol. 23, No. 17, 1982, pages 1847-1850). This reagent can be thought of as a milder version of potassium permanganate and while it has similar uses it produces products in much higher yields without all that pesky overoxidation of the product that makes KMnO4 so useless for organic chem. Given how easy BPSP is to make and how widely available the reactants needed to make it are I have no doubt that it will prove to be a useful addition to any amateur chemists toolkit.

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Download Paper (if this link doesn't work go to the website and type in the name of the paper "Bispyridinesilver Permanganate [Ag(C5H2N)2]: An Efficient Oxidizing Reagent For Organic Substrates"):
https://sci-hub.se/10.1016/s0040-4039(00)86758-1

I meant to have a link to where you could download the Encyclopedia of Reagents for Organic Synthesis but when I went to get the link I found out that the zlibrary has deleted it! :'( I have a copy so if anyone wants to see the data for the rest of the reactions email me at [email protected] and I will send you some screen shots.

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This video documents my experimentation with the famous pyro mix that can be ignited with a couple drops of water. I had trouble getting it to work consistently at first but I was able to figure out what the problem was and the final result was pretty cool. Even the failures produced something interesting: a plastic-like compound that actually resists dissolving in water to the point that it can survive days of rainfall more or less intact. This experiment came from a textbook (I try not to look at other videos on experiments I want to do), the Preparatory Manual of Black Powder and Pyrotechnics (link to free download below).

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Download Textbook: https://b-ok.cc/book/913872/11f64f

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In this video I prepare copper sulfamate from sulfamic acid and copper carbonate. This procedure is very easy to carry out and it can be done with cobalt or nickel to produce their sulfamates in a more or less identical manner. The prep comes from Inorganic Laboratory Preparations pages 39-40.

Download Inorganic Laboratory Preparations ebook for free:
https://b-ok.cc/book/666160/f02534
Sulfamic Acid on Sciencemadness Wiki
http://www.sciencemadness.org/smwiki/index.php/Sulfamic_acid

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In this video I try a prep from ILP of sodium manganate(V) which contains the turquoise colored hypomanganate ion (FINALLY a light blue that isn't hideous! YAY!). The compound is unstable and even if the prep works perfectly storing it is problematic. I could not find any real uses for this compound so I made it just as a curiosity so that we could see what it looks like. I do offer numerous suggestions on how the prep could be improved in case someone wants to absolutely not repeat it. ;-)

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In this video I prepare dinitrotetrapyridinenickel(II) as described on pages 193-194 of Inorganic Laboratory Preparations, a textbook that I have taken many preps from for this channel. It is very similar to the dinitrotetraaminenickel(II) I made several months ago which comes from the same textbook. In theory any small primary or secondary amine should be able to make compounds of this general type.

Download the textbook Inorganic Laboratory Preparations free:
https://1lib.us/book/666160/f02534
Preparation of Dinitrotetraaminenickel(II):
https://www.youtube.com/watch?v=GNHdWMJ0uak

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In this video I synthesize barium manganate from manganese dioxide, potassium hydroxide, and barium nitrate. The prep is pretty simple and straightforward. Supposedly barium manganate can be used to carry out a whole laundry list of oxidations in which alcohols are converted to aldehydes and ketones in excellent yields.

SciHub: https://sci-hub.se/

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In this video I give my thoughts on a popular method used to extract freebase DMT from various plant sources and why it's a bad extraction method. I do this purely for purposes of harm reduction and education. I do not now nor have I ever condoned anyone manufacturing controlled substances for any reason.

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It used to be that wanting to have your own chemistry lab was seen as respectable and taking personal agency for your own practical education was regarded as being noble (because they are). These days we have a bunch of pearl clutching snobs that think that the unwashed masses shouldn't do chemistry because they don't have degrees. This is nothing more than intellectual elitism and supreme arrogance. I have degrees too. They don't make you special. And if you get hurt that is 100% on you. Chemistry is dangerous though I strongly suspect you already know this.

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In this video I make up blueish-black rubidium triiodide from rubidium iodide and elemental iodine using methanol as a solvent. This process would work to make sodium, potassium, cesium, and thallium(I) triiodides as well. Presumably it would also work for lithium as well although I have not checked that one.

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In this two part series I repeat the process of producing “crystal kratom” from kratom leaf powder. Also included are many of the basic tenets of acid-base extractions; so much so that this video could be considered a general guide to all alkaloid extractions amenable to simple extractions of this type. If there is any way to make it easier to understand I really cannot think of what it is. At some point you just have to jump in and get your hands dirty. If you screw it up then start over and do it again. I didn't get to this point with this extraction by just thinking or reading about it. You cannot expect to either. There is no such thing as being an “armchair chemist”.

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In this two part series I repeat the process of producing “crystal kratom” from kratom leaf powder. Also included are many of the basic tenets of acid-base extractions; so much so that this video could be considered a general guide to all alkaloid extractions amenable to simple extractions of this type. If there is any way to make it easier to understand I really cannot think of what it is. At some point you just have to jump in and get your hands dirty. If you screw it up then start over and do it again. I didn't get to this point with this extraction by just thinking or reading about it. You cannot expect to either. There is no such thing as being an “armchair chemist”.

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In this video I prepare silver chlorate from silver nitrate using a process I found in Inorganic Syntheses, Volume 2. It is a very simple metathesis reaction that just about anyone could do. Silver chlorate is pretty sensitive to light but it's not as bad as silver chloride.

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Synthesis Protocol on PoorMansChemist Website:
http://www.poormanschemist.com/PMC_Blog/PMC_Blog.html
Inorganic Syntheses, Volume 2 Ebook:
https://b-ok.cc/book/564297/6c8da0
Buy High Quality Silver Nitrate on eBay:
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In this very short video I show you my first test of an old mix used to create a purple colored flame. The mixture contains potassium chlorate, calomel, strontium nitrate, and cupric oxide. The original formulation also called for shellac but both it and its popular substitute (red gum) were sold out on Fireworks Cookbook. So I tried it with gum arabic instead. Clearly that was a bad choice. But this experiment confirms that I am on the right track to achieving a pure purple flame and what I learned from the attempt will allow me to formulate a mix that burns continuously. Not knowing what the smoke contains I am going overboard with the safety on this one and will only do the second attempt when the wind is blowing back towards the woods consistently and it's late at night so there is no chance whatsoever of anyone being in any danger at all.

Composition Recipe at Fireworks Cookbook:
https://fireworkscookbook.com/firework-recipe/g-w-purple-pill-box-chlorate/

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In this video I prepare barium perchlorate from ammonium perchlorate. The process used results in a pretty pure compound that is suitable for use in preparing pure perchloric acid by a metathesis reaction between barium perchlorate and dilute sulfuric acid. The barium sulfate is filtered off and the perchloric acid is concentrated normally by evaporation.

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Synthesis of Barium Chlorate From Potassium Chlorate
https://www.bitchute.com/video/YFOO0ePLTB9f/
Explosives Laboratory (I know, it's a YT channel but they are worth checking out):
https://www.youtube.com/channel/UCDC0WqWmwa77KkORQwa3ylQ

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In this video I demonstrate the process of recycling silver metal using nitric acid, sodium chloride, sodium hydroxide, and common table sugar (sucrose).

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In this video I attempt to make "germanium ultramarine", a compound that I have seen described in two whole sentences on atomistry. The results that I was able to get even with my primitive set-up were quite remarkable. Not 100% sure exactly what is going on in this but maybe someone who has a kiln will watch this video and give the experiment a proper try. If you do PLEASE share the result with us!!!

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I apologize this took so long to upload. I think BitChute is a little overwhelmed at the moment. In this video I try using arsenic to color a flame white as was done in the days before things like powdered aluminum. This mix produces arsenic trioxide laden smoke so it should not be repeated by anyone.

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In this video I demonstrate an excellent green fire composition. I also set chunks of lithium metal on fire with a blowtorch on the wooden bench top for the hell of it. The rest was quite spectacular.

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n this video I prepare sodium nitroprusside a.k.a. Sodium Nitrosyl Cyanoferrate from potassium ferrocyanide and 43% nitric acid. You can see the entire prep written out step by step on my website (link below) along with 65 other preps in my personal library of synthesis procedures (I'm always adding more as I have time).

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Prep of Sodium Nitroprusside on poormanschemist.com
http://www.poormanschemist.com/PMC_Grimoire/PMC_Grimoire.html#nitroprusside
Sodium Nitroprusside Crystals Under the Microscope:
https://www.youtube.com/watch?v=5F_COZUZQSw

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My thoughts on current events, big tech censorship, and a message to those who are ready to take on the deep state tyrannical and illegitimate government. Violence is a tactical mistake and is not the way to go. Instead we should focus on organizing and popularizing peaceful but adamant refusal to comply and civil disobedience. Violent action is what the enemy wants and when your enemy wants you to do a thing it is vital that you do not do that thing.

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In this video I dissolve ytterbium and calcium metals in liquid anhydrous ammonia and play around with the pyrophoric ytterbium amide. Making this video was a stupid amount of fun. :-)

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In this video I prepare an obscure compound, Cs2[BiI5]. The source for this prep comes from a Wikipedia article on cesium chloride which references an older Russian work. Apparently many years ago (and perhaps still today) the quantitative precipitation of cesium salts was used in analytical chemistry to identify various metals cations and oxycations. These days most analytical work in labs is done with very expensive instrumentation that most hobby chemists simply don't have access too. However, these older analytical techniques still work just as well today as they did in the past and can be a powerful addition to the amateur chemists analytical toolkit. Plus they are colorful and fun to make.

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Wikipedia, Cesium Chloride, Analytical Chemistry Section:
https://en.wikipedia.org/wiki/Caesium_chloride#Analytical_chemistry
A Much Better Color Coded List of The Reactions From the Wikipedia Page Above:
http://www.poormanschemist.com/PMC_Grimoire/PMC_Grimoire.html#cesiumsalt
On the Composition of the Cesium Salt by KBiI4 Reagent:
https://core.ac.uk/download/pdf/39208249.pdf
7:05 Preparation of Bismuth Nitrate and Bismuth Trioxide From the Metal
https://www.youtube.com/watch?v=mTx2UK9xy2g&t=1166s

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In this video prepare a double salt of terbium sulfate and investigate its fluorescent properties. As it turns out the double salt fluoresces just as well as plain terbium sulfate does but the color is different. Whereas terbium sulfate fluoresces a green color rubidium terbium sulfate is more of a yellow color. This prep is very easy and all of the chemcal involved range from low toxicity to non-toxic. The 1.5M H2SO4 is the most dangerous thing in the entire prep. This would be a great experient for beginners and for homeschoolers.

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0:45 myst32YT's Terbium Sulfate Video:
https://www.youtube.com/watch?v=DJcObFauFIc
Sciencemadness Wiki Terbium Sulfate:
http://www.sciencemadness.org/smwiki/index.php/Terbium_sulfate
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5:27 Converting Rb/Cs Chloride to Other Salts:
https://www.youtube.com/watch?v=2MXWBNiSiag&list=PLkBtGo4CFTHoWs8KLnS01PfNytwCLJfjx

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Created 1 year, 6 months ago.

181 videos

Category Science & Technology

On this channel I focus on making rarely seen chemical compounds and demonstrating other laboratory procedures in my back yard chem lab. Unlike many home chemists I am not big on boom compounds. Instead I like to focus on those elements and compounds best described as "wildly poisonous" that other chemists hesitate to play with. I have a Bachelors degree in chem so yes I do know what I am doing. Although much of my stuff is not really meant for other amateur chemists to repeat (especially not a beginner!!!) I am very active in the amateur/hobby chemistry and I try to be as supportive of amateur chemists as I possibly can.
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