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Reduction of Barium Nitrate to Barium Nitrite Using Freshly Made Lead Sponge

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First published at 19:10 UTC on July 18th, 2020.

poormanschemist

PoorMansChemist

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In this video I generate lead sponge by the reaction of a solution of lead(II) acetate with magnesium ribbon. The lead sponge is then boiled with a solution of barium nitrate to produce barium nitrite and lead monoxide. The barium nitrite is then purified to obtain the final product. My final product didn't look stellar but it may have been the barium nitrate I used to do the synthesis. Regardless I think it worked. :-) Confirmation of refutation will be posted later. Suggestions for easy tests for nitrite ion are most welcome!

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Procedure taken from Inorganic Laboratory Preparations pages 34-35
Textbook Free Download: https://b-ok.cc/book/666160/f02534
Synthesis Protocol: poormanschemist.com/PMC_Grimoire/PMC_Grimoire.html#bano2

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