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TERT-PENTYL ALCOHOL SYNTHESIS grignard reaction PART 3

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First published at 03:25 UTC on March 5th, 2019.

#tert
#pentyl
#grignard

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I finish drying and then distill and then put the lower fraction back in a dean stark apparatus but found NO WATER. I wanted to then distill the lower fraction a second time but screw it. If i had i would have lost another 10 mL taking me from a 66% to a 50% yield. With an overall yield of 66% the average yield between the grignard reagent reaction and the actual grignard reaction would be 81% yield for each reaction. AT LEAST I IMPROVED

LESS