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Synthesis of Antimony(III) Iodide From Antimony & Iodine

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First published at 22:29 UTC on October 15th, 2019.

#chemistry
#antimony
#iodide

poormanschemist

PoorMansChemist

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In this video I demonstrate the synthesis of antimony(III) iodide from ground antimony metal and iodine in toluene. The protocol for this synthesis was taken from the Handbook of Preparative Inorganic Chemistry, 2nd Edition, Volume 1, page 614. You can find more information about this compound and its chemistry on atomistry.com at the link below. SbI3 reacts with water to produce antimony oxyiodide. This can be difficult to clean off glassware but it will dissolve in strong HCl quite readily.

Errata: At 14:30 the subtitle should read "Her condition degraded over months until by the end she appeared to be in agony although her docs said they didn't think she could even feel pain anymore."

Atomistry.com SbI3 Page: http://antimony.atomistry.com/antimon...

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