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Synthesis of Praseodymium(III,IV) Oxide From Praseodymium Metal

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First published at 12:38 UTC on October 13th, 2019.

poormanschemist

PoorMansChemist

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In this video I demonstrate the synthesis of a lanthanide oxide by thermal decomposition of its oxalate salt using praseodymium. We start off with praseodymium metal and convert that into Pr(III)Cl3 by reacting the metal with HCl. The chloride is then converted into the oxalate which is filtered off and dried. The dry oxalate powder is then put into a crucible and heated until all of the oxalate has converted to the oxide.

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