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Benzylmagnesium chloride synthesis. BzMgCl C6H5CH2MgCl grignard reagent P2P

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First published at 22:34 UTC on April 23rd, 2020.

BlueDex1

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Synthesis of benzylmagnesium chloride. BzMgCl C6H5CH2MgCl grignard reagent.

A crystal of iodine, 4.8 g of magnesium sawdust is placed in a flask and a solution of 25.4 g of benzyl chloride in 75ml of absolute ether is gradually added dropwise. After the introduction of 1/4 of the solution, the reaction should begin, followed by boiling ether. If the reaction has not begun, it can be caused by substituting a cup of warm water under the flask. The course of the reaction should be regulated by cooling and changing the rate of prilipanie benzyl chloride.

If P2P is desired, dry distilled toluene can be added and acetonitrile can be added. The ether/toluene mixture is ideal for acetonitrile grignard reaction. Hydrolysis would yield phenylacetone.

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Benzylmagnesium chloride synthesis. BzMgCl C6H5CH2MgCl grignard reagent P2P

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